caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; N,N-dimethyl-formamide
T=50°C; Suzuki reaction; 2 h; Title compound not separated from byproducts;
参考文献
Oh, Chang Ho; Lim, Young Mook; You, Choong Ho
Tetrahedron Letters, 2002 , vol. 43, # 26 p. 4645 - 4648
1: ortho-bromo-phenol With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78°C; 0.5 h;
2: With zinc(II) chloride in tetrahydrofuran; pentane
T=20°C; 1 h;
3: 4-bromo-1-iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane
T=20°C; 24 h; Further stages.;
