(i) NaH, DMSO, (ii) /BRN= 506746/; Multistep reaction;
参考文献
Mitsui,S. et al.
Tetrahedron, 1973 , vol. 29, p. 1523 - 1530
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Klein,J.; Lichtenberg,D.
Journal of Organic Chemistry, 1970 , vol. 35, p. 2654 - 2656
anhydrous ammonium carbonate in ethanol
T=55 - 60°C;
参考文献
Palacin, Serge; Chin, Donovan N.; Simanek, Eric E.; MacDonald, John C.; Whitesides, George M.; McBride, Mary T.; Palmore, G. Tayhas R.
Journal of the American Chemical Society, 1997 , vol. 119, # 49 p. 11807 - 11816