3,4-二甲氧基硫代苯甲酰胺合成路线 （共 15 条）
反应条件
pyridine; hydrogen sulfide; triethylamine 6 h; Ambient temperature;
参考文献
Khadse, B. G.; Lokhande, S. R.; Bhamaria, R. P.; Prabhu, S. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 856 - 860
反应条件
methanesulfonic acid T=30°C; 5.3 h;
参考文献
Aki, Shinji; Fujioka, Takafumi; Ishigami, Masashi; Minamikawa, Jun-ichi
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 17 p. 2317 - 2320
反应条件
in hydrochloric acid-DMF; diethyl ether; water
反应条件
1: 88.4 percent / NH2OH*HCl, sodium hydroxide / aq. ethanol; H2O / 3 h / Ambient temperature 2: 78.5 percent / acetic anhydride / 0.5 h / Heating 3: 75 percent / hydrogen sulphide gas, triethylamine, pyridine / 6 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 856 - 860
反应条件
1: 78.5 percent / acetic anhydride / 0.5 h / Heating 2: 75 percent / hydrogen sulphide gas, triethylamine, pyridine / 6 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 856 - 860
反应条件
in ethanol 8 h; Irradiation;
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 103, # 2 p. 259 - 270
反应条件
potassium hydroxide; benzo-15-crown-5; methyl iodide in 1,4-dioxane T=20 - 25°C; 3 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 39, # 8 p. 998 - 1001
反应条件
1: aq. KOH / dioxane / 4.5 h / 20 - 25 °C 2: 27 percent / aq. KOH; benzo-15-crown-5 / dioxane / 3 h / 40 - 45 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 39, # 8 p. 998 - 1001
反应条件
potassium hydroxide; benzo-15-crown-5; methyl iodide in 1,4-dioxane T=20 - 25°C; 3 h;
参考文献
Sayfullina; Tashmukhamedova; Shakhidoyatov
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 8 p. 998 - 1001
反应条件
1: aq. KOH / dioxane / 4.5 h / 20 - 25 °C 2: 65 percent / aq. KOH / dioxane / 3 h / 20 - 25 °C View Scheme
参考文献
Sayfullina; Tashmukhamedova; Shakhidoyatov
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 8 p. 998 - 1001
