6-甲氧基-3,4-二氢-2H-1,4-苯并噁嗪合成路线 （共 4 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C;
参考文献
Vermeulen, Erik S; van Smeden, Marjan; Schmidt, Anne W; Sprouse, Jeffrey S; Wikstroem, Hakan V; Grol, Cor J
Journal of medicinal chemistry, 2004 , vol. 47, # 22 p. 5451 - 5466
反应条件
1: 98 percent / H2 / Pd/C / ethanol / 0.33 h / 20 °C / 1810.02 Torr 2: 87 percent / K2CO3 / acetonitrile / 2 h / Heating 3: 91 percent / LiAlH4 / tetrahydrofuran / 20 °C View Scheme
参考文献
Journal of medicinal chemistry, , vol. 47, # 22 p. 5451 - 5466
反应条件
potassium carbonate in N,N-dimethyl-formamide T=125°C; 15 h;
参考文献
Tetrahedron Letters, , vol. 47, # 44 p. 7823 - 7826
反应条件
1: 87 percent / K2CO3 / acetonitrile / 2 h / Heating 2: 91 percent / LiAlH4 / tetrahydrofuran / 20 °C View Scheme
参考文献
Journal of medicinal chemistry, , vol. 47, # 22 p. 5451 - 5466
