1,4,7-三氮环壬烷 三盐酸盐合成路线 （共 4 条）
反应条件
1: With sulfuric acid T=100°C; 72 h; Inert atmosphere; 2: With sodium hydroxide in water Inert atmosphere; 3: With hydrogenchloride in water pH=1;
参考文献
Eitel, Simon H.; Bauer, Matthias; Schweinfurth, David; Deibel, Naina; Sarkar, Biprajit; Kelm, Harald; Krueger, Hans-Joerg; Frey, Wolfgang; Peters, Rene
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4683 - 4693
反应条件
sodium hydroxide in water; toluene Heating;
参考文献
Stavila, Vitalie; Allali, Mustapha; Canaple, Laurence; Stortz, Yvon; Franc, Cecile; Maurin, Philippe; Beuf, Olivier; Dufay, Olivier; Samarut, Jacques; Janier, Marc; Hasserodt, Jens
New Journal of Chemistry, 2008 , vol. 32, # 3 p. 428 - 435
反应条件
lithium hydroxide hydrate in water
T=45°C; pH=10; Reflux;
参考文献
Majkowska-Pilip; Bilewicz
Journal of Inorganic Biochemistry, 2011 , vol. 105, # 2 p. 313 - 320
反应条件
1: sodium hydroxide / water / pH 12
2: sodium carbonate / 24 h / 50 °C / |Inert atmosphere
3: trifluoroacetic acid / 24 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Maheshwari, Vidhi; Dearling, Jason L.J.; Treves, S. Ted; Packard, Alan B.
Inorganica Chimica Acta, 2012 , vol. 393, p. 318 - 323
