4-氯-4'-甲氧基联苯合成路线 (共 62 条)
反应条件
hydrogen bromide; acetic acid
参考文献
Dewar; James
Journal of the Chemical Society, 1958 , p. 917,921
反应条件
C43H54N2S; palladium diacetate; potassium carbonate in water; isopropyl alcohol
T=100°C; Suzuki-Miyaura coupling reaction; 4 h; Aerobic conditionSealed tube;
参考文献
Li, Hong-Ling; Wu, Zhi-Sheng; Yang, Min; Qi, Yan-Xing
Catalysis Letters, 2010 , vol. 137, # 1-2 p. 69 - 73
反应条件
sodium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate; palladium diacetate
T=100°C; Suzuki coupling reaction; 0.5 h;
参考文献
Xin, Bingwei; Zhang, Yuhong; Liu, Leifang; Wang, Yanguang
Synlett, 2005 , # 20 art. no. W02205ST, p. 3083 - 3086
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tert.-butylnitrite; trifuran-2-yl-phosphane; acetic acid in N,N-dimethyl-formamide
T=90°C; 8 h; Inert atmosphere;
参考文献
Mo, Fanyang; Qiu, Di; Jiang, Yubo; Zhang, Yan; Wang, Jianbo
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 518 - 522
反应条件
potassium carbonate; [PS-PEG-adppp-Pd(η3-C3H5)]Cl in water
T=50°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Uozumi, Yasuhiro; Nakai, Yasushi
Organic Letters, 2002 , vol. 4, # 17 p. 2997 - 3000
反应条件
C28H38Cl2N2O6PdS2(2-)*2Na(1+); potassium carbonate in ethanol; water
T=70°C; Suzuki coupling;
参考文献
Zhou, Jin; Guo, Xuming; Tu, Changzheng; Li, Xiaoyan; Sun, Hongjian
Journal of Organometallic Chemistry, 2009 , vol. 694, # 5 p. 697 - 702
反应条件
C21H15ClN2O2Pd; potassium carbonate in isopropyl alcohol
T=50°C; Suzuki-Miyaura Coupling; 2 h;
参考文献
Dewan, Anindita; Bora, Utpal; Borah, Geetika
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1689 - 1692
反应条件
1: (4-Chlorophenyl)-boronic acid With iodine; potassium carbonate in acetonitrile
T=80°C; 9 h; Inert atmosphereSchlenk techniqueSealed tube;
2: (4-methoxyphenyl)-boronic acid With palladium diacetate in acetonitrile
T=80°C; Suzuki Coupling; 15 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Niu, Liting; Zhang, Hao; Yang, Haijun; Fu, Hua
Synlett, 2014 , vol. 25, # 7 art. no. 691, p. 995 - 1000
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water
T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
反应条件
boron trifluoride diethyl etherate; palladium diacetate in 1,4-dioxane
T=20°C; Suzuki coupling; 10 h; Inert atmosphere; chemoselective reaction;
参考文献
Nan, Guangming; Zhu, Fanghua; Wei, Zhijun
Chinese Journal of Chemistry, 2011 , vol. 29, # 1 p. 72 - 78