4-氯-4'-甲氧基联苯合成路线 (共 62 条)
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
palladium diacetate in tetrahydrofuran
T=20°C; Stille reaction; 1.75 h;
参考文献
Dughera, Stefano
Synthesis, 2006 , # 7 p. 1117 - 1122
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=20°C; 0.0833333 h;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano; Giaveno, Cinzia
European Journal of Organic Chemistry, 2006 , # 21 p. 4884 - 4890
反应条件
1: hexakis-(4-chloro-phenyl)-cyclotrisiloxane With potassium hydroxide in 1,4-dioxane; water
Heating;
2: 1-bromo-4-methoxy-benzene With palladium diacetate in 1,4-dioxane; water
4 h; Heating; Further stages.;
参考文献
Endo, Mayuko; Sakurai, Tomoyuki; Ojima, Satoshi; Katayama, Takako; Unno, Masafumi; Matsumoto, Hideyuki; Kowase, Susumu; Sano, Hiroshi; Kosugi, Masanori; Fugami, Keigo
Synlett, 2007 , # 5 p. 749 - 752
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
triphenylphosphine; Pd bipyridyl anchored nanosized mesoporous silica MCM-41 in tetrahydrofuran
Kumada-Corriu reaction; 48 h; Heating;
参考文献
Tsai, Fu-Yu; Lin, Bo-Nan; Chen, Ming-Jie; Mou, Chung-Yuan; Liu, Shiuh-Tzung
Tetrahedron, 2007 , vol. 63, # 20 p. 4304 - 4309
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide
T=60°C; Stille coupling; 8 h;
参考文献
Zhao, Hong; Wang, Yue; Sha, Junchao; Sheng, Shouri; Cai, Mingzhong
Tetrahedron, 2008 , vol. 64, # 32 p. 7517 - 7523
反应条件
palladium diacetate; potassium carbonate in butanone
T=120°C; Ullmann reaction; 12 h; Inert atmosphere;
参考文献
Wang, Liqiang; Lu, Wenjun
Organic Letters, 2009 , vol. 11, # 5 p. 1079 - 1082
反应条件
palladium 10 on activated carbon; tetrabutyl ammonium fluoride; water; tris(p-fluoro phenyl)phosphine in toluene
T=120°C; Hiyama coupling; 9 h; Inert atmosphere;
参考文献
Yanase, Takayoshi; Mori, Shigeki; Monguchi, Yasunari; Sajiki, Hironao
Chemistry Letters, 2011 , vol. 40, # 9 p. 910 - 912
反应条件
potassium fluoride in dimethyl sulfoxide
T=105°C; 2 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Huang, Dan-Feng
European Journal of Organic Chemistry, 2010 , # 3 p. 416 - 419