4-氯-4'-甲氧基联苯合成路线 （共 62 条）
反应条件
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in acetonitrile
T=20°C; Suzuki cross-coupling; 48 h; Inert atmosphere;
参考文献
Proutiere, Fabien; Schoenebeck, Franziska
Angewandte Chemie - International Edition, 2011 , vol. 50, # 35 p. 8192 - 8195
反应条件
alginate/gellan gum beads containing Pd nanoparticles in water
T=40°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Cacchi, Sandro; Caponetti, Eugenio; Casadei, Maria Antonietta; Di Giulio, Andrea; Fabrizi, Giancarlo; Forte, Giovanni; Goggiamani, Antonella; Moreno, Sandra; Paolicelli, Patrizia; Petrucci, Francesco; Prastaro, Alessandro; Saladino, Maria Luisa
Green Chemistry, 2012 , vol. 14, # 2 p. 317 - 320
反应条件
palladium diacetate; potassium carbonate in methanol
T=60°C; Suzuki Coupling; Inert atmosphere;
参考文献
Liu, Jin-Biao; Yan, Hui; Chen, Hui-Xuan; Luo, Yu; Weng, Jiang; Lu, Gui
Chemical Communications, 2013 , vol. 49, # 46 p. 5268 - 5270
反应条件
tetrabutyl ammonium fluoride; acetic acid in toluene
T=100°C; Hiyama Coupling; 24 h;
参考文献
Huang, Shao-Hsien; Liu, Chun-Hsia; Yang, Chia-Min
Green Chemistry, 2014 , vol. 16, # 5 p. 2706 - 2712
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium methylate in ethylene glycol dimethyl ether; water
T=50°C; 5 h;
参考文献
Kang; Hong; Kim; Lee
Journal of Chemical Research - Part S, 2001 , # 7 p. 283 - 285
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine; silver(l) oxide in methanol
Suzuki-Miyaura cross-coupling reaction; 1.5 h; Heating;
参考文献
Cella, Rodrigo; Cunha, Rodrigo L. O. R.; Reis, Ana E. S.; Pimenta, Daniel C.; Klitzke, Clecio F.; Stefani, Helio A.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 244 - 250
反应条件
potassium carbonate; triphenylphosphine in methanol
T=50°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Masuyama, Yoshiro; Sugioka, Yutaka; Chonan, Shiori; Suzuki, Noriyuki; Fujita, Masahiro; Hara, Kenji; Fukuoka, Atsushi
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 352, p. 81 - 85
反应条件
1: 4-methoxy-aniline With tert.-butylnitrite; boron trifluoride diethyl etherate in methanol
T=0°C; 0.5 h; Schlenk technique;
2: (4-Chlorophenyl)-boronic acid in methanol
T=0 - 60°C; 5 h; Schlenk technique;
参考文献
Zong, Yan; Hu, Jiefeng; Sun, Peipei; Jiang, Xiaoqing
Synlett, 2012 , vol. 23, # 16 art. no. ST-2012-W0506-L, p. 2393 - 2396
反应条件
copper(l) iodide; RhCl(PPh3)4; potassium carbonate in anhydrous xylene
T=130°C;
参考文献
Wang, Jingjing; Chen, Weiqiang; Zuo, Sujing; Liu, Lu; Zhang, Xinrui; Wang, Jianhui
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12334 - 12338
Angew. Chem., 2012 , vol. 124, # 49 p. 12500 - 12504,5
反应条件
iodine
5 h; Heating;
参考文献
Tamura, Yasumitsu; Yoshimoto, Yoshihiko; Tada, Shin-ichi; Kunimoto, Katsutoshi; Matsumura, Shingo; et al.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 8 p. 1006 - 1010
