5-苯甲酰基呋喃-2-甲酸甲酯合成路线 （共 7 条）
反应条件
iron(III) chloride in dichloromethane 36 h; Heating;
参考文献
Kuo, Sheng-Chu; Lee, Fang-Yu; Teng, Che-Ming; Huang, Li-Jiau; Chou, Li-Chen; Guh, Jih-Hwa; Pan, Shiow-Lin
Patent: US2005/215612 A1, 2005 ;
Location in patent: Page/Page column 3; 5 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate; potassium iodide in various solvent(s) T=80°C; P=760 Torr; 16 h;
参考文献
Ishiyama, Tatsuo; Kizaki, Hiroe; Hayashi, Takahiro; Suzuki, Akira; Miyaura, Norio
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4726 - 4731
反应条件
anhydrous iron chloride in dichloromethane T=20°C;
参考文献
US2010/130556 A1, ;
Page/Page column 20 ;
反应条件
aluminium trichloride T=50 - 60°C; Acylation; 0.25 h;
参考文献
Belen'kii; Gromova; Kolotaev; Krayushkin
Chemistry of Heterocyclic Compounds, 2000 , vol. 36, # 3 p. 256 - 263
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=84°C; Acylation; 0.416667 h; Title compound not separated from byproducts;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 36, # 3 p. 256 - 263
反应条件
water; sodium hydroxide in tetrahydrofuran T=20°C;
参考文献
Yin, Biao-Lin; Lai, Jin-Qiang; Zhang, Ze-Ren; Jiang, Huan-Feng
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1961 - 1965
反应条件
1.1: acetic acid / methanol / Heating 2.1: Pb(OAc)4 / CH2Cl2 / 0.5 h / 30 °C 2.2: BF3*Et2O / CH2Cl2 / 0.5 h / Heating 3.1: 87 percent / calcium borohydride / tetrahydrofuran / 6 h / Heating View Scheme
参考文献
Le; Lien; Huang; Tsai; Teng; Wu; Cheng; Kuo
Journal of Medicinal Chemistry, 2001 , vol. 44, # 22 p. 3746 - 3749
