反应条件
1: 60 percent / chromous chloride / acetone / 1 h / 20 °C
2: 99 percent / trifluoroacetic acid
3: 59 percent / K2CO3 / butan-2-one / 6 h / Heating
4: 1.) borane, 2.) NaOH, 30percent H2O2 / 1.) THF, 20 deg C, 15 min, 2.) 20 deg C, 15 min
5: 1.) AlCl3, 2.) conc. HCl / 1.) nitrobenzene, room temperature, 12 h, 2.) water, 20 deg C, 7 d
View Scheme
参考文献
Gupta, Dharmendra N.; Hodge, Philip; Khan, Naeem
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 689 - 696
