2-(4-甲基噻唑-5-基)乙胺合成路线 （共 11 条）
反应条件
hydrogen; Lindlar's catalyst in methanol P=760 Torr; 2.5 h;
参考文献
Islam, Imadul; Ng, Ka-yun; Chong, Kong Teck; McQuade, Thomas J.; Hui, John O.; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 2 p. 293 - 304
反应条件
ethanol; nickel P=2206.5 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1067
反应条件
1: 54 percent / ZnN6-pyridine2, PPh3, diisopropyl azodicarboxylate / toluene / 3 h / Ambient temperature 2: 97 percent / H2 / Pd/CaCO3 / methanol / 2.5 h / 760 Torr View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 2 p. 293 - 304
反应条件
1: POCl3 / 120 °C 2: palladium/ZrO2; acetic acid; HCl / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1067
反应条件
1: aqueous NH3 2: POCl3 / 120 °C 3: palladium/ZrO2; acetic acid; HCl / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1067
反应条件
ueber das Hydrazid und Azid;
参考文献
US2139570 , ;
DE704236 , ;
DRP/DRBP Org.Chem.
反应条件
potassium hydroxide; bromine anschliessend Erhitzen mit KOH;
参考文献
US2139570 , ;
DE704236 , ;
DRP/DRBP Org.Chem.
参考文献
Journal of the Chemical Society, , p. 443,445
反应条件
1: dimethylformamide / (heating) 2: (i) N2H4*H2O, (ii) aq. HCl View Scheme
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 33, p. 3723 - 3725,3655 - 3657
反应条件
(i) N2H4*H2O, (ii) aq. HCl; Multistep reaction;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 33, p. 3723 - 3725,3655 - 3657
