1-(苯并[d][1,3]二氧代l-5-基)-N,N-二甲基甲胺合成路线 （共 15 条）
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 15, p. 171
反应条件
1: 1.) n-BuLi / 1.) THF, 0 deg C, 2.) -78 deg C 2: 98 percent / (i-Pr)2EtN / dimethylformamide 3: 99 percent / ClCO2Et / tetrahydrofuran / 25 °C 4: 1.) Mg / 2.) THF 5: 93 percent / 1 N H2SO4 / tetrahydrofuran / 25 °C 6: 40 percent / I2, PPh3, DIPEA 7: 70 percent / AgClO4 / acetonitrile / 25 °C 8: 61 percent / methanol / Irradiation View Scheme
参考文献
Narasimhan, N. S.; Mali, R. S.; Kulkarni, B. K.
Tetrahedron, 1983 , vol. 39, # 12 p. 1975 - 1982
参考文献
Tiffeneau; Fuhrer
Bulletin de la Societe Chimique de France, 1914 , vol. <4> 15, p. 171
反应条件
NiCuFeO(x) in anhydrous xylene
24 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
sodium hydroxide in diethyl ether
T=-6°C; 1.83333 h;
参考文献
Cushman, Mark; Choong, Tung-Chung; Valko, Joseph T.; Koleck, Mary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5067 - 5073
反应条件
1: With titanium(IV) isopropylate; triethylamine in ethanol
T=25°C; 12 h;
2: With sodium tetrahydroborate in ethanol
T=25°C; 10 h; Further stages.;
参考文献
Cai, Guixin; Fu, Ye; Li, Yizhou; Wan, Xiaobing; Shi, Zhangjie
Journal of the American Chemical Society, 2007 , vol. 129, # 24 p. 7666 - 7673
参考文献
Dai-Ho, Ginny; Mariano, Patrick S.
Journal of Organic Chemistry, 1987 , vol. 52, # 4 p. 704 - 706
反应条件
formaldehyd
T=80°C; 24 h;
参考文献
Dai-Ho; Mariano
Journal of Organic Chemistry, 1988 , vol. 53, # 21 p. 5113 - 5127
反应条件
formic acid
T=190°C; 6 h;
参考文献
Sharma, M. L.; Kapoor, J. L.; Sood, Nirupma; Kaur, Satwinder; Kalsi, P. S.
Journal of the Indian Chemical Society, 1986 , vol. 63, p. 682 - 684
反应条件
sodium cyanoborohydride; zinc(II) chloride
1 h;
参考文献
Cutter, Paul S; Miller, R.Bryan; Schore, Neil E
Tetrahedron, 2002 , vol. 58, # 8 p. 1471 - 1478
