1-(苯并[d][1,3]二氧代l-5-基)-N,N-二甲基甲胺合成路线 （共 15 条）
反应条件
1: 100 percent / H2O / 3 h / 23 °C
2: LiALH4 / diethyl ether / 1.17 h / Heating
3: 65 percent / (aq) NaOH / diethyl ether / 1.83 h / -6 °C
View Scheme
参考文献
Cushman, Mark; Choong, Tung-Chung; Valko, Joseph T.; Koleck, Mary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5067 - 5073
反应条件
1: LiALH4 / diethyl ether / 1.17 h / Heating
2: 65 percent / (aq) NaOH / diethyl ether / 1.83 h / -6 °C
View Scheme
参考文献
Cushman, Mark; Choong, Tung-Chung; Valko, Joseph T.; Koleck, Mary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 25 p. 5067 - 5073
反应条件
hydrogen in hexane
T=170°C; 48 h;
参考文献
Cui, Xinjiang; Dai, Xingchao; Zhang, Yan; Deng, Youquan; Shi, Feng
Chemical Science, 2014 , vol. 5, # 2 p. 649 - 655
反应条件
1: hydrogen chloride
2: im Rohr
View Scheme
参考文献
Tiffeneau
Bulletin de la Societe Chimique de France, 1911 , vol. <4> 9, p. 932
参考文献
Tiffeneau
Bulletin de la Societe Chimique de France, 1911 , vol. <4> 9, p. 932
