2,3-二巯基-1-丙醇合成路线 （共 30 条）
反应条件
1: With sulfur; ethanolamine; hydrazine in water T=70 - 73°C; 2.5 h; 2: 2,3-dibromo-propan-1-ol With ethanolamine; hydrazine in water T=45 - 50°C; 2 h; 3: With potassium hydroxide; hydrazine in water T=80°C; 2 h; Inert atmosphere;
参考文献
Levanova; Grabel'nykh; Sukhomazova; Zemirova; Russavskaya; Albanov; Klyba; Zhanchipova; Korchevin
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 10 p. 1428 - 1433
反应条件
1: With sulfur; ethanolamine; hydrazine in water T=60 - 65°C; 2 h; 2: epichlorohydrin With ethanolamine; hydrazine in water T=22°C; 3 h; 3: With potassium hydroxide; hydrazine in water T=80°C; 2 h; Inert atmosphere;
参考文献
Russian Journal of Organic Chemistry, , vol. 44, # 10 p. 1428 - 1433
反应条件
methanol; sodium hydrogensulfide T=70 - 80°C;
参考文献
Journal of the Chemical Society, , p. 1394
反应条件
dibenzoyl peroxide Irradiation.UV-Licht; Behandeln des Reaktionsprodukts mit wss.-methanol.Salzsaeure;
参考文献
Journal of Organic Chemistry, , vol. 23, p. 551,553
反应条件
ethanol; phenylhydrazine
参考文献
Bulletin of the Chemical Society of Japan, , vol. 30, p. 455,457
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2413 - 2416
反应条件
T=60 - 70°C; P=5148.6 Torr;
参考文献
Journal of the Chemical Society, , p. 247
参考文献
Journal of the Chemical Society, , p. 247
参考文献
Journal of the Chemical Society, , p. 817,824
