1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane T=-50°C; Metallation; 0.5 h; 2: With water-d2 in tetrahydrofuran; hexane Substitution;
参考文献
Mongin, Florence; Trecourt, Francois; Queguiner, Guy
Tetrahedron Letters, 1999 , vol. 40, # 30 p. 5483 - 5486
1: 38 percent / DCC / tetrahydrofuran / Ambient temperature 2: dimethylformamide / 120 h / Ambient temperature View Scheme
参考文献
Acosta, C. Kirk; Bahr, Martin L.; Burdett, James E.; Cessac, James W.; Martinez, Rudy A.; et al.
Journal of Chemical Research, Miniprint, 1991 , # 5 p. 914 - 934