P(C6H5)3 in toluene (Ar); to a soln. of Ni(COD)2 Ph3P is added, to this mixt. BrCH2CN is added; pptn with n-hexane, ppt. is filtered off, washed with n-hexane, elem. anal.;
参考文献
Wilhelm, D.; Hoffmann, T.; Wenschuh, E.; Reck, G.; Winter, G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1993 , vol. 619, p. 1801 - 1806
caesium carbonate in acetonitrile T=0 - 20°C; Inert atmosphere;
参考文献
UNIVERSITY OF PITTSBURGH-OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION
Patent: WO2009/139886 A2, 2009 ;
Location in patent: Page/Page column 47 ;
WO 2009/139886 A2
