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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
顺-2-丁烯
合成路线
（共 370 条）
106-98-9
1-丁烯
+
590-18-1
顺-2-丁烯
+
624-64-6
反-2-丁烯
+
71-43-2
苯
→
反应条件
1013-03-2
+
135-98-8
仲丁基苯
+
6565-55-5
+
61064-05-9
+
1014-41-1
1,4-二(丁烷-2-基)苯
反应条件
specimen (I) T=50°C; Product distribution;
参考文献
Russian Journal of Physical Chemistry, , vol. 54, # 2 p. 276 - 277
Zhurnal Fizicheskoi Khimii, , vol. 54, # 2 p. 480 - 482
106-98-9
1-丁烯
+
590-18-1
顺-2-丁烯
+
624-64-6
反-2-丁烯
+
71-43-2
苯
→
反应条件
1013-03-2
+
135-98-8
仲丁基苯
+
61064-05-9
+
1014-41-1
1,4-二(丁烷-2-基)苯
+
1079-96-5
反应条件
specimen (II) T=50°C; Product distribution;
参考文献
Russian Journal of Physical Chemistry, , vol. 54, # 2 p. 276 - 277
Zhurnal Fizicheskoi Khimii, , vol. 54, # 2 p. 480 - 482
590-18-1
顺-2-丁烯
+
74-90-8
+
106-99-0
→
反应条件
25899-50-7
+
26294-98-4
+
16529-66-1
+
20068-02-4
+
30574-97-1
+
592-51-8
+
16529-56-9
+
100-40-3
+
16545-78-1
反应条件
C48H52O4P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=99.84°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/73171 A1, 2005 ;
Location in patent: Page/Page column 38-41; sheet 6 ;
590-18-1
顺-2-丁烯
+
74-90-8
+
106-99-0
→
反应条件
106-98-9
1-丁烯
+
25899-50-7
+
26294-98-4
+
16529-66-1
+
20068-02-4
+
30574-97-1
+
592-51-8
+
16529-56-9
+
4553-62-2
+
100-40-3
+
16545-78-1
反应条件
1: With C48H52O4P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=83.84°C; 2: T=119.84°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/73174 A1, 2005 ;
Location in patent: Page/Page column 76-80; sheet 3 ;
590-18-1
顺-2-丁烯
+
74-90-8
+
111-69-3
+
106-99-0
→
反应条件
25899-50-7
+
26294-98-4
+
16529-66-1
+
20068-02-4
+
30574-97-1
+
592-51-8
+
16529-56-9
+
4553-62-2
+
100-40-3
+
16545-78-1
反应条件
1: With C42H40O6P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=99.84°C; 2: With nickel T=109.84°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/73174 A1, 2005 ;
Location in patent: Page/Page column 86-89; sheet 4 ;
590-18-1
顺-2-丁烯
+
74-90-8
+
106-99-0
→
反应条件
25899-50-7
+
26294-98-4
+
16529-66-1
+
20068-02-4
+
30574-97-1
+
592-51-8
+
16529-56-9
+
4553-62-2
+
100-40-3
+
16545-78-1
反应条件
1: With C44H44O6P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=99.84°C; 2: With Lewis acid T=109.84°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/73171 A1, 2005 ;
Location in patent: Page/Page column 32-35; sheet 4 ;
590-18-1
顺-2-丁烯
+
74-90-8
+
111-69-3
+
4553-62-2
+
106-99-0
→
反应条件
25899-50-7
+
26294-98-4
+
16529-66-1
+
20068-02-4
+
30574-97-1
+
592-51-8
+
16529-56-9
+
100-40-3
+
16545-78-1
反应条件
C48H52O4P2; (m-tolyl-O-)(p-tolyl-O-)2P; (m-tolyl-O-)2(p-tolyl-O-)P; tri(m-methylphenyl) phosphite; tri-p-tolyl phosphite T=89.84°C; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2005/73174 A1, 2005 ;
Location in patent: Page/Page column 89-91; sheet 5 ;
106-98-9
1-丁烯
+
590-18-1
顺-2-丁烯
+
624-64-6
反-2-丁烯
+
75-28-5
+
463-82-1
+
96-37-7
+
106-97-8
→
反应条件
62016-28-8
+
108-08-7
+
591-76-4
+
560-21-4
+
565-75-3
+
540-84-1
+
592-13-2
+
921-47-1
+
7154-80-5
+
20278-85-7
+
4032-93-3
+
14720-74-2
+
565-59-3
+
584-94-1
+
589-43-5
+
78-78-4
+
96-14-0
+
107-83-5
+
79-29-8
+
464-06-2
+
2213-23-2
+
1072-05-5
+
3522-94-9
+
110-82-7
反应条件
sulfuric acid in water T=1.65666°C; P=2963.34 Torr; Product distribution / selectivity;
参考文献
Catalytic Distillation Technologies
Patent: US2007/299292 A1, 2007 ;
Location in patent: Page/Page column 7 ;
590-18-1
顺-2-丁烯
→
反应条件
13317-63-0
反应条件
Me2S*BH2Br in dichloromethane T=25°C; 1 h;
参考文献
Brown,H.C. et al.
Journal of Organic Chemistry, 1979 , vol. 44, # 14 p. 2417 - 2422
106-98-9
1-丁烯
+
590-18-1
顺-2-丁烯
+
624-64-6
反-2-丁烯
+
75-28-5
+
463-82-1
+
96-37-7
+
106-97-8
→
反应条件
62016-28-8
+
108-08-7
+
591-76-4
+
560-21-4
+
565-75-3
+
540-84-1
+
592-13-2
+
921-47-1
+
7154-80-5
+
20278-85-7
+
4032-93-3
+
14720-74-2
+
565-59-3
+
584-94-1
+
589-43-5
+
78-78-4
+
96-14-0
+
107-83-5
+
79-29-8
+
464-06-2
+
2213-23-2
+
1072-05-5
+
3522-94-9
+
110-82-7
反应条件
sulfuric acid in water T=1.65666°C; P=2963.34 Torr; Product distribution / selectivity;
参考文献
Catalytic Distillation Technologies
Patent: US2007/299292 A1, 2007 ;
Location in patent: Page/Page column 7 ;
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