4,4-二甲基-2-戊酮合成路线 （共 111 条）
反应条件
1: NaOBr
2: PCl3; bromine / 60 - 70 °C / dann auf 100grad
View Scheme
参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
反应条件
potassium chlorate; bromine
参考文献
Thorpe,J.W.; Warkentin,J.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 927 - 935
参考文献
Greene,F.D. et al.
Journal of Organic Chemistry, 1963 , vol. 28, p. 55 - 64
反应条件
1: NaOBr
2: SOCl2
3: auf dem Dampfbad
View Scheme
参考文献
Homeyer; Whitmore; Wallingford
Journal of the American Chemical Society, 1933 , vol. 55, p. 4209,4212
参考文献
Thorpe,J.W.; Warkentin,J.
Canadian Journal of Chemistry, 1973 , vol. 51, p. 927 - 935
反应条件
1: diethyl ether
2: CuSO4; pumice stone / 200 °C / Hydrieren des entstandenen Olefingemisches in Gegenwart von Nickel-Kieselgur bei 120-135grad und 120 at
View Scheme
参考文献
Moersch; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 820
反应条件
sodium ethanolate
unter Abdestillieren des freigesetzten Aethanols;
参考文献
Sanofi-Synthelabo
Patent: US2005/182104 A1, 2005 ;
Location in patent: Page/Page column 7 ;
反应条件
1: methanol; aqueous sulfuric acid
2: concentrated aqueous hydrochloric acid
View Scheme
参考文献
Graham et al.
Journal of the Chemical Society, 1954 , p. 2180,2190
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791
Full Text Show Details
Moersch; Whitmore
Journal of the American Chemical Society, 1949 , vol. 71, p. 820
Full Text Show Details
Whitmore; Rohrmann
Journal of the American Chemical Society, 1941 , vol. 63, p. 2034
参考文献
Whitmore et al.
Journal of the American Chemical Society, 1938 , vol. 60, p. 2462,2791
