5-巯基-1,2,3-三氮唑单钠盐合成路线 （共 3 条）
反应条件
pyridine in dichloromethane; 1-chloro-1,1-difluoro-methane
参考文献
Bristol-Myers Company
Patent: US4714760 A1, 1987 ;
Title/Abstract Full Text Show Details
Bristol-Myers Company
Patent: US4868294 A1, 1989 ;
反应条件
pyridine; methanol 1.) freon TF, CH2Cl2, from 0 to 5 deg C, 30 min, 2.) from 0 to 5 deg, 10 min; Yield given. Multistep reaction;
参考文献
Walker, Donald G.; Brodfuehrer, Paul R.; Brundidge, Steven P.; Shih, Kun Mao; Sapino, Chester
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 983 - 991
反应条件
pyridine; methanol 1.) CH2Cl2, 2.) from 0 to 5 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Walker, Donald G.; Brodfuehrer, Paul R.; Brundidge, Steven P.; Shih, Kun Mao; Sapino, Chester
Journal of Organic Chemistry, 1988 , vol. 53, # 5 p. 983 - 991
