tetrakis(triphenylphosphine) palladium(0) in DMF (N,N-dimethyl-formamide)
T=80°C; 3 h;
参考文献
Jacobsen, Eric Jon; Myers, Jason K.; Walker, Daniel Patrick; Wishka, Donn G.; Reitz, Steven Charles; Piotrowski, David W.; Acker, Brad A.; Groppi JR., Vincent E.
Patent: US2003/236270 A1, 2003 ;
Location in patent: Page 39 ;
1: With potassium hydroxide; water in ethanol
72 h; Heating / reflux;
2: With hydrogenchloride in ethanol; water
pH=< 2;
参考文献
Jacobsen, Eric Jon; Myers, Jason K.; Walker, Daniel Patrick; Wishka, Donn G.; Reitz, Steven Charles; Piotrowski, David W.; Acker, Brad A.; Groppi JR., Vincent E.
Patent: US2003/236270 A1, 2003 ;
Location in patent: Page 39 ;
