(S)-1-(吡啶-2-基)乙醇合成路线 (共 24 条)
反应条件
1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -70 °C 2: tetrabutylammonium fluoride / CH2Cl2; tetrahydrofuran / 20 h / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 43, # 6 p. 1151 - 1158
参考文献
Helvetica Chimica Acta, , vol. 38, p. 1114,1116
反应条件
titanium(III) chloride; acetic acid; acetone 3 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 39, # 8 p. 1239 - 1246
反应条件
titanium(III) chloride; acetic acid 3 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 39, # 8 p. 1239 - 1246
反应条件
titanium(III) chloride; acetic acid 3 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 39, # 8 p. 1239 - 1246
反应条件
sulfuric acid 1 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 55, # 9 p. 2906 - 2910
反应条件
1: 1.) n-BuLi 2: NaBH4 View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 43 p. 7973 - 7976
反应条件
hydrogenchloride; bis-[(trifluoroacetoxy)iodo]benzene 1.) CH2Cl2, r.t., 1 h, 2.) ether; Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 43, # 6 p. 1151 - 1158
反应条件
dihydrogen peroxide; trifluoroacetic acid; Fe(II)(O2CCF3)2(py)4 Oxidation; Substitution; Product distribution; Further Variations:Reaction partners;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 13 p. 2343 - 2346
反应条件
trimethyltelluronium iodide 1.) hexane, THF, -60 deg C, 10 min, 2.) -78 deg C -> RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 2847 - 2848