1-(4-甲基苯甲酰)-1H-苯并三唑合成路线 (共 31 条)
反应条件
sodium azide; FeCl3·6H2O in water; acetone T=20°C; 0.166667 h;
参考文献
Zhong, Zhiyun; Hu, Jieling; Wang, Xiaoxia; Liu, Junhua; Zhang, Longfeng
Synthetic Communications, 2011 , vol. 41, # 16 p. 2461 - 2467
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.5 h;
参考文献
Singh, Kamal Nain; Kaur, Amarjit
Synthetic Communications, 2005 , vol. 35, # 22 p. 2935 - 2937
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Tetrahedron Letters, 2002 , vol. 43, # 31 p. 5431 - 5433
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 0.0833333 h;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Tetrahedron, 2003 , vol. 59, # 23 p. 4201 - 4207
反应条件
in tetrahydrofuran T=20°C; 4 h;
参考文献
Katritzky; He; Suzuki
Journal of Organic Chemistry, 2000 , vol. 65, # 24 p. 8210 - 8213
反应条件
1: ethyl acetoacetate With sodium hydride in tetrahydrofuran T=20°C; 0.666667 h; 2: 4-MeC6H4COBt in tetrahydrofuran T=20°C; 14 h; 3: With ammonium hydroxide; ammonium chloride in tetrahydrofuran; water 1 h; Heating;
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Wilkerson, Chavon R.; Hall, C. Dennis; Akhmedov, Novruz G.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6617 - 6622
反应条件
1: acetonitrile With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: 4-MeC6H4COBt in tetrahydrofuran; hexane T=-78°C; 2 h;
参考文献
Katritzky, Alan R.; Abdel-Fattah, Ashraf A. A.; Wang, Mingyi
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4932 - 4934
反应条件
T=330°C; P=0.045004 Torr; 0.25 h; Product distribution; Further Variations:TemperaturesPressures;
参考文献
Tetrahedron, , vol. 61, # 34 p. 8257 - 8263
反应条件
in water T=70°C; 1 h; Microwave irradiationGreen chemistry;
参考文献
Panda, Siva S.; Ibrahim, Mohamed A.; Oliferenko, Alexander A.; Asiri, Abdullah M.; Katritzky, Alan R.
Green Chemistry, 2013 , vol. 15, # 10 p. 2709 - 2712
反应条件
T=600°C; P=0.2 Torr; 2.77778E-06 h; Product distribution; Further Variations:TemperaturesPressures;
参考文献
Tetrahedron, , vol. 61, # 34 p. 8257 - 8263