1-(4-甲基苯甲酰)-1H-苯并三唑合成路线 （共 31 条）
反应条件
in chloroform
T=25°C; 12 h;
参考文献
Katritzky, Alan R.; Cai, Chunming; Suzuki, Kazuyuki; Singh, Sandeep K.
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 811 - 814
反应条件
1.1: iPr2NLi / tetrahydrofuran / 1.75 h / -78 °C
1.2: 58 percent / tetrahydrofuran / -78 - 20 °C
2.1: 77 percent / toluene / 0.5 h / Heating
View Scheme
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Hall, C. Dennis; Suzuki, Kazuyuki
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4854 - 4856
反应条件
samarium; titanium tetrachloride in tetrahydrofuran
24 h; Heating;
参考文献
Wang, Xiaoxia; Zhang, Yongmin
Synthetic Communications, 2003 , vol. 33, # 15 p. 2627 - 2634
反应条件
in chloroform
T=80°C; 0.166667 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Singh, Sandeep K.
Journal of Organic Chemistry, 2006 , vol. 71, # 9 p. 3375 - 3380
反应条件
titanium tetrachloride in dichloromethane
T=25°C; 2 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.; He, Hai-Ying
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5720 - 5723
反应条件
1: acetylacetone With sodium hydride in tetrahydrofuran
T=20°C; 0.666667 h;
2: 4-MeC6H4COBt in tetrahydrofuran
T=20°C; 14 h;
3: With ammonium hydroxide; ammonium chloride in tetrahydrofuran; water
1 h; Heating;
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Wilkerson, Chavon R.; Hall, C. Dennis; Akhmedov, Novruz G.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6617 - 6622
反应条件
1: acetylacetone With sodium hydride in tetrahydrofuran
T=20°C; 0.666667 h;
2: (1H-benzo[d][1,2,3]triazol-1-yl)(furan-2-yl)methanone; 4-MeC6H4COBt in tetrahydrofuran
T=20°C; 14 h;
3: With ammonium hydroxide; ammonium chloride in tetrahydrofuran; water
1 h; Heating;
参考文献
Katritzky, Alan R.; Wang, Zuoquan; Wang, Mingyi; Wilkerson, Chavon R.; Hall, C. Dennis; Akhmedov, Novruz G.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6617 - 6622
反应条件
1: nitromethane With potassium tert-butylate in dimethyl sulfoxide
T=16°C; 0.166667 h; Inert atmosphere;
2: 4-MeC6H4COBt in dimethyl sulfoxide
T=20°C; 17 h;
参考文献
Takamoto, Mikihiro; Kurouchi, Hiroaki; Otani, Yuko; Ohwada, Tomohiko
Synthesis, 2009 , # 24 art. no. F13909SS, p. 4129 - 4136
反应条件
titanium tetrachloride in dichloromethane
T=25°C; 2 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.; He, Hai-Ying
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5720 - 5723
反应条件
zinc dibromide in dichloromethane
3 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.; He, Hai-Ying
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5720 - 5723
