Power, David P.; Lozach, Olivier; Meijer, Laurent; Grayson, David H.; Connon, Stephen J.
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 16 p. 4940 - 4944
sodium hydroxide; tetra(n-butyl)ammonium hydroxide in tetrahydrofuran; water
1 h;
参考文献
Dalton, Lesley; Humphrey, Godfred L.; Cooper, Melanie M.; Joule, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2417 - 2422
Dalton, Lesley; Humphrey, Godfred L.; Cooper, Melanie M.; Joule, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2417 - 2422
1: 1134 mg / NaOH, tetra-n-butylammonium hydroxide / tetrahydrofuran; H2O / 1 h
2: 420 mg / H2 / 5percent Pd-C / ethanol / 12 h / 60 °C / 2280 Torr
3: 240 mg / pyridine / 4 h / Ambient temperature
View Scheme
参考文献
Dalton, Lesley; Humphrey, Godfred L.; Cooper, Melanie M.; Joule, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2417 - 2422
Dalton, Lesley; Humphrey, Godfred L.; Cooper, Melanie M.; Joule, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2417 - 2422
1: 1134 mg / NaOH, tetra-n-butylammonium hydroxide / tetrahydrofuran; H2O / 1 h
2: 420 mg / H2 / 5percent Pd-C / ethanol / 12 h / 60 °C / 2280 Torr
3: 240 mg / pyridine / 4 h / Ambient temperature
4: 4 mg / NaH / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Dalton, Lesley; Humphrey, Godfred L.; Cooper, Melanie M.; Joule, John A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2417 - 2422