氘代3-羟基-3-甲基(D3)合成路线 （共 3 条）
反应条件
acetic anhydride 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2989 - 2993
反应条件
sulfuric acid; dihydrogen peroxide; oxygen; ozone
1) ethyl acetate, -78 deg C; 2) H2O, 2 h, reflux; Yield given. Multistep reaction;
参考文献
Gill, Harjit K.; Smith, Roland W.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2989 - 2993
反应条件
1: 76 percent / acetic anhydride / 18 h
2: 42 percent / NaBH4 / propan-2-ol / 24 h / Ambient temperature
View Scheme
参考文献
Gill, Harjit K.; Smith, Roland W.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 11 p. 2989 - 2993
