1: 5,5'-(2-thioxo-1,3-dithide-4,5-diyl) bis(benzenecarbothiate) With sodium methylate in methanol
T=20°C; 0.5 h;
2: propyl bromide in methanol
T=20°C; 2 h;
参考文献
Kimura, Shinya; Kurai, Hiroyuki; Mori, Takehiko; Mori, Hatsumi; Tanaka, Shoji
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 1 p. 59 - 65
1: carbon disulfide With sodium in N,N-dimethyl-formamide
8 h; Inert atmosphereCooling;
2: With tetraethylammonium bromide; ammonia; zinc(II) chloride in water
T=20°C; 0.5 h;
3: propyl bromide Further stages;
参考文献
Rivadehi, Shadi; Reid, Ellen F.; Hogan, Conor F.; Bhosale, Sheshanath V.; Langford, Steven J.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 705 - 709
