2-甲基-n-苯基丙氨酸合成路线 (共 11 条)
反应条件
hydrogen; palladium on activated charcoal in methanol
24 h; Ambient temperature; Yield given;
参考文献
Sasaki, Tadashi; Mori, Kohki; Ohno, Masatomi
Synthesis, 1985 , # 3 p. 280 - 282
反应条件
1: CHCl3 / 12 h / Ambient temperature
2: H2 / 10percent Pd/C / methanol / 24 h / Ambient temperature
View Scheme
参考文献
Sasaki, Tadashi; Mori, Kohki; Ohno, Masatomi
Synthesis, 1985 , # 3 p. 280 - 282
反应条件
hydroxylamine in methanol
T=60°C; 18 h; xanthone production by hydrolysis (CH3COOH, H2SO4, H2O, reflux, 14 h); Product distribution;
参考文献
Hafiz, Mushtag; Taylor, Giles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1700 - 1705
反应条件
hydrogenchloride
T=160°C;
参考文献
Iwakura,Y. et al.
Tetrahedron, 1968 , vol. 24, p. 575 - 583
反应条件
1: diethyl ether / beim Schuetteln in der Kaelte
2: concentrated hydrochloric acid
View Scheme
参考文献
Bucherer; Grolee
Chemische Berichte, 1906 , vol. 39, p. 992
参考文献
Banti
Gazzetta Chimica Italiana, 1929 , vol. 59, p. 824
参考文献
Bucherer; Grolee
Chemische Berichte, 1906 , vol. 39, p. 992
反应条件
1: diethyl ether
2: concentrated hydrochloric acid
View Scheme
参考文献
Bucherer; Grolee
Chemische Berichte, 1906 , vol. 39, p. 992
反应条件
potassium hydroxide; ethanol
参考文献
Banti
Gazzetta Chimica Italiana, 1929 , vol. 59, p. 824
反应条件
T=160°C; Verseifen des erhaltenen Estergemisches;
参考文献
Bischoff; Mintz
Chemische Berichte, 1892 , vol. 25, p. 2324