tetra-n-butylammonium tetrafluoroborate; Ni(cyclam)Br2 in N,N-dimethyl-formamide
T=20°C; Carboxylation; cyclization; P=760 Torr; ElectrolysisMg/Ni electrodes; Product distribution; Further Variations:CatalystsPressuresReaction partnersnature of the electrodes;
参考文献
Olivero; Dunach
European Journal of Organic Chemistry, 1999 , # 8 p. 1885 - 1891
1: 84 percent / K2CO3 / dimethylformamide / 21 h / Ambient temperature
2: 19 percent / 0.5 h / 650 °C / 0 Torr
View Scheme
参考文献
Black, Michael; Cadogan, J. I. G.; McNab, Hamish
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 2 p. 155 - 160
Ye, Tao; Garcia, Concepcion Fernandez; McKervey, M. Anthony
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 11 p. 1373 - 1380
Das, Suresh; Rajesh, C. S.; Thanulingam, T. L.; Ramaiah, D.; George, M. V.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1545 - 1548