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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-溴甲基苯
合成路线
（共 404 条）
591-17-3
3-溴甲基苯
+
1122-93-6
4-甲氧基苯酚钾
→
反应条件
82721-04-8
反应条件
copper
参考文献
Ungnade; Rubin
Journal of Organic Chemistry, 1951 , vol. 16, p. 1311,1313
288-13-1
吡唑
+
591-17-3
3-溴甲基苯
→
反应条件
850380-23-3
反应条件
copper(l) iodide; manganese(II) fluoride; (1R,2R)-(-)-trans-1,2-diaminocyclohexane; potassium hydroxide in water T=100°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Lim, Gina Shiyun
Tetrahedron Letters, 2011 , vol. 52, # 52 p. 7171 - 7174
591-17-3
3-溴甲基苯
→
反应条件
85566-04-7
反应条件
1: 80 percent / Mg / diethyl ether; benzene / 1.) 0 deg C up to RT; 2.) RT, 1 h 2: 100 percent / sodium dichromate / acetic acid / 70 h / Heating 3: 80 percent / aq. KOH, KMnO4 / 1.5 h / Heating 4: 100 percent / thionyl chloride / 8 h / Heating 5: 78 percent / AlCl3 / 1.) 0 deg C up to RT; 2.) RT, 3 h 6: 79 percent / hydrazine hydrate / ethanol / 40 h / Heating 7: 45 percent / MnO2, KOH / diethyl ether; ethanol / 1.5 h / dark View Scheme
参考文献
Teki, Yoshio; Takui, Takeji; Itoh, Koichi; Iwamura, Hiizu; Kobayashi, Kazumasa
Journal of the American Chemical Society, 1986 , vol. 108, # 9 p. 2147 - 2156
591-17-3
3-溴甲基苯
+
66-25-1
正己醛
→
反应条件
88226-72-6
反应条件
pyrrolidine; 1,3-bis-(diphenylphosphino)propane; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide T=115°C; Heck reaction; 6 h; Molecular sieve;
参考文献
Ruan, Jiwu; Saidi, Ourida; Iggo, Jonathan A.; Xiao, Jianliang
Journal of the American Chemical Society, 2008 , vol. 130, # 32 p. 10510 - 10511
591-17-3
3-溴甲基苯
+
56-35-9
→
反应条件
68971-88-0
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere; regioselective reaction;
参考文献
Gerbino, Dario C.; Fidelibus, Pablo M.; Mandolesi, Sandra D.; Ocampo, Romina A.; Scoccia, Jimena; Podesta, Julio C.
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 24 - 32
591-17-3
3-溴甲基苯
+
1461-22-9
→
反应条件
68971-88-0
反应条件
magnesium; ethylene dibromide in tetrahydrofuran T=35°C; Barbier Coupling Reaction; 1 h; SonicationInert atmosphere; regioselective reaction;
参考文献
Gerbino, Dario C.; Fidelibus, Pablo M.; Mandolesi, Sandra D.; Ocampo, Romina A.; Scoccia, Jimena; Podesta, Julio C.
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 24 - 32
591-17-3
3-溴甲基苯
→
反应条件
69120-23-6
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexanes / -78 °C / Inert atmosphere 1.2: -78 - 30 °C / Inert atmosphere 2.1: silver(I) acetate; palladium diacetate / 1,2-dichloro-ethane / 5 h / 80 °C / Inert atmosphere 3.1: silver fluoride / methanol / 20 °C / Inert atmosphere; Darkness View Scheme
参考文献
Huang, Chunhui; Chernyak, Natalia; Dudnik, Alexander S.; Gevorgyan, Vladimir
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 8 p. 1285 - 1305
67-56-1
+
591-17-3
3-溴甲基苯
+
68-12-2
→
反应条件
6935-65-5
+
99-36-5
反应条件
1: 1-bromo-3-methyl-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
591-17-3
3-溴甲基苯
+
118486-94-5
→
反应条件
89929-89-5
反应条件
1,4-diaza-bicyclo[2.2.2]octane; Pd0(tris(tert-butyl)phosphine)2; sodium chloride in water T=20°C; Stille Cross Coupling; 4 h; Inert atmosphere;
参考文献
Lu, Guo-Ping; Cai, Chun; Lipshutz, Bruce H.
Green Chemistry, 2013 , vol. 15, # 1 p. 105 - 109
110-00-9
+
591-17-3
3-溴甲基苯
→
反应条件
89929-89-5
反应条件
Yield given. Multistep reaction;
参考文献
Pelter, Andrew; Rowlands, Martin; Clements, Gillian
Synthesis, 1987 , # 1 p. 51 - 53
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