magnesium in diethyl ether
Ar atmosphere. addn. of bromide to soln. of Mg, reflux (2 h), addn. of soln. of Sn compound, reflux (2 h); removement of solvent;
参考文献
Niestroj, Michael; Lube, Andreas; Neumann, Wilhelm P.
Chemische Berichte, 1995 , vol. 128, # 6 p. 575 - 580
1: 1-bromo-3-methyl-benzene With magnesium in tetrahydrofuran
3 h; Heating;
2: 9,10-Dichloroanthracene With Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=50 - 60°C;
