1: ammonium thiocyanate With benzoyl chloride in acetone HeatingReflux; 2: 3-bromo-aniline in acetone HeatingRefluxCooling with ice; 3: With hydrogenchloride; ammonia; sodium hydroxide in water T=80°C; pH=10; Cooling with ice;
参考文献
THE BOARD OF TRUSTEES OF THE LELAND STANFORD JUNIOR UNIVERSITY; AUCKLAND UNISERVICES LIMITED
Patent: WO2009/114552 A1, 2009 ;
Location in patent: Page/Page column 144 ;