反应条件
1: triethylamine / dichloromethane / 0 °C / Inert atmosphere 2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 °C 4: diisobutylaluminium hydride / tetrahydrofuran; n-heptane / 4.5 h / -78 - 0 °C / Inert atmosphere 5: triethylamine / dichloromethane / 0 °C / Inert atmosphere 6: lithium triethylborohydride / tetrahydrofuran / -30 - 20 °C / Inert atmosphere 7: palladium 10 on activated carbon; hydrogen / methanol / 1500.15 Torr 8: dibromo-difluoro-methane; tert-butyl alcohol / dichloromethane / 1.5 h / 60 °C / Inert atmosphere; Microwave irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 134, # 33 p. 13592 - 13595
