1: iodobenzene; REM resin With PhP(CH2CH2C6F13)2; triethylamine; palladium diacetate in carbon dioxide T=100°C; Heck reaction; 40 h; 2: methanol With sodium methylate in tetrahydrofuran Further stages.;
参考文献
Early; Gordon; Carroll; Holmes; Shute; McConvey
Chemical Communications, 2001 , # 19 p. 1966 - 1967
tris(dibenzylideneacetone)dipalladium (0); triphenyl-arsane in tetrahydrofuran T=50°C; 18 h; Yields of byproduct given;
参考文献
Busacca, Carl A.; Swestock, John; Johnson, Robert E.; Bailey, Thomas R.; Musza, Laszlo; Rodger, Charles A.
Journal of Organic Chemistry, 1994 , vol. 59, # 24 p. 7553 - 7556