2,2,3,3-四甲基氮丙啶合成路线 （共 3 条）
反应条件
water; triphenylphosphine in tetrahydrofuran
24 h; Ambient temperature;
参考文献
Lion, Claude; Boukou-Poba, Jean-Paul; Saumtally, Imran
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 9 p. 711 - 718
反应条件
toluene-4-sulfonic acid in methanol-d4
T=20°C; 24 h; Title compound not separated from byproducts.;
参考文献
Chukanov; Popov; Romanenko; Reznikova
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1227 - 1233
反应条件
1: 89 percent / NBS, NaN3 / 1,2-dimethoxy-ethane; H2O / 2 h / 0 °C
2: 71 percent / PPh3, H2O / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Lion, Claude; Boukou-Poba, Jean-Paul; Saumtally, Imran
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 9 p. 711 - 718
