1,4,5,8,9,10-六氢蒽合成路线 (共 10 条)
反应条件
sodium in tetrahydrofuran; ethanol; ammonia T=-78°C; 12 h;
参考文献
Mehta, Goverdhan; Sen, Saikat; Ramesh, Senaiar S.
European Journal of Organic Chemistry, 2007 , # 3 p. 423 - 436
反应条件
lithium in tetrahydrofuran; ammonia 4 h;
参考文献
Journal of the American Chemical Society, , vol. 102, p. 637
反应条件
white sand; calcium; tert-butyl alcohol in tetrahydrofuran; ethylenediamine T=0°C; 24 h; Yield given;
参考文献
Benkeser, Robert A.; Laugal, James A.; Rappa, Angela
Tetrahedron Letters, 1984 , vol. 25, # 20 p. 2089 - 2092
反应条件
tetra(n-butyl)ammonium hydroxide in water T=80°C; electrolysis, 10 F/mol, divided cell;
参考文献
Tetrahedron, , vol. 42, # 8 p. 2185 - 2192
反应条件
lithium; methylamine
参考文献
Angewandte Chemie, , vol. 78, p. 642 - 643
反应条件
lithium; tert-butyl alcohol Heating;
参考文献
Justus Liebigs Annalen der Chemie, , p. 1406 - 1415
反应条件
1.) electrolysis, 2.1M tetrabutylammonium hydroxide, 80 deg C, divided cell, 10 F/mol, 2.) reflux, 48 h; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 42, # 8 p. 2185 - 2192
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 42, # 8 p. 2185 - 2192
反应条件
1.) electrolysis, 2.1M tetrabutylammonium hydroxide, 80 deg C, 2.) reflux, 48 h; different electrolytic cells; Product distribution;
参考文献
Tetrahedron, , vol. 42, # 8 p. 2185 - 2192
反应条件
Wilkinson's catalyst; hydrogen
参考文献
Birch,A.J.; Walker,K.A.M.
Australian Journal of Chemistry, 1971 , vol. 24, p. 513 - 520