(E,E)-2,4-壬二烯醛合成路线 （共 23 条）
反应条件
hydrogenchloride in tetrahydrofuran Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 683 - 690
反应条件
1: CrO3*2Py / CH2Cl2 2: (i) NaH, THF, (ii) /BRN= 1700822/ 3: LiAlH4, AlCl3 / diethyl ether 4: CrO3*2Py / CH2Cl2 View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 32, p. 627 - 634
反应条件
1: LiAlH4, AlCl3 / diethyl ether 2: CrO3*2Py / CH2Cl2 View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 32, p. 627 - 634
反应条件
tetrahydrofuran Behandeln der Reaktionsloesung mit Aethanol und mit Lithiumalanat und anschliessenden Behandeln mit wss.Schwefelsaeure;
参考文献
Journal of Organic Chemistry, , vol. 23, p. 1580
反应条件
in tetrahydrofuran T=-78°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 683 - 690
反应条件
in tetrahydrofuran T=-78°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 683 - 690
反应条件
1: LiAlH4
2: NEt3 / diethyl ether / Ambient temperature
View Scheme
参考文献
Ishii, Youichi; Gao, Chao; Xu, Wen-Xiang; Iwasaki, Masakazu; Hidai, Masanobu
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6818 - 6825
反应条件
triethylsilane; oxygen; lt;5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinatogt;cobalt(II) in dichloromethane; isopropyl alcohol
T=28°C; P=760 Torr; 1.5 h;
参考文献
Sugamoto, Kazuhiro; Matsushita, Yoh-Ichi; Matsui, Takanao
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 23 p. 3989 - 3998
反应条件
triethylsilane; lt;5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinatogt;cobalt(II); oxygen; phosphorous acid trimethyl ester
1.) 2-propanol, CH2Cl2, 28 deg C, 1.5 h, 1 atm, 2.) 2-propanol, CH2Cl2, 2 h, r.t.; Yield given. Multistep reaction;
参考文献
Matsushita; Matsushita, Yoh-Ichi; Sugamoto; Sugamoto, Kazuhiro; Nakama; Nakama, Tuyoshi; Sakamoto; Sakamoto, Toshifumi; Matsui; Matsui, Takanao; Nakayama; Nakayama, Mitsuru
Tetrahedron Letters, 1995 , vol. 36, # 11 p. 1879 - 1882
反应条件
silica gel in benzene
20 h; Heatingdark;
参考文献
Fujii; Nakamura; Yasui; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 7 p. 2423 - 2427
