(E,E)-2,4-壬二烯醛合成路线 （共 23 条）
反应条件
(i) NaOMe, DMF, (ii) /BRN= 1702396/; Multistep reaction;
参考文献
Bergel'son,L.D. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 611 - 614
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 683 - 687
反应条件
1: 83 percent / tetrahydrofuran
2: 74 percent / H2 / (methyl benzoate)chromium tricarbonyl / acetone / 3 h / 120 - 125 °C / 45600 Torr
3: 71 percent / propionic acid / toluene / 3 h / Heating
4: 76 percent / LiAlH4 / diethyl ether
5: 88 percent / pyridine
View Scheme
参考文献
Vasil'ev; Serebryakov
Russian Chemical Bulletin, 1996 , vol. 45, # 9 p. 2232 - 2235
反应条件
1: 83 percent / tetrahydrofuran
2: 74 percent / H2 / (methyl benzoate)chromium tricarbonyl / acetone / 3 h / 120 - 125 °C / 45600 Torr
3: 71 percent / propionic acid / toluene / 3 h / Heating
4: 76 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Vasil'ev; Serebryakov
Russian Chemical Bulletin, 1996 , vol. 45, # 9 p. 2232 - 2235
