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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
5912-82-3
合成路线
（共 14 条）
1427318-51-1
+
676-58-4
甲基氯化镁
→
反应条件
5912-82-3
反应条件
NiCl2(PPh3)2 in tetrahydrofuran T=20°C; 12 h; Inert atmosphere;
参考文献
Yang, Zhaozhen; Chen, Xiaoyi; Kong, Wei; Xia, Siyuan; Zheng, Renwei; Luo, Fang; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 13 p. 2175 - 2185
→
反应条件
5912-82-3
反应条件
NiCl2((PPh3)P)2 in tetrahydrofuran T=20°C; 10 h; Inert atmosphere;
参考文献
Liu, Ge; Kong, Lichun; Shen, Ji; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 14 p. 2310 - 2321
2327-99-3
丙-1,2-二烯基苯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5912-82-3
反应条件
acetic acid; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane 5 h; Heating;
参考文献
Guo, Hao; Ma, Shengming
Synthesis, 2007 , # 17 p. 2731 - 2745
122948-71-4
+
1589-82-8
苄基溴化镁
→
反应条件
5912-82-3
反应条件
[NiI2(PPh3)]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=70°C; Kumada Cross-Coupling; Inert atmosphere; chemoselective reaction;
参考文献
Wu, Ji-Cheng; Gong, Lu-Bing; Xia, Yuanzhi; Song, Ren-Jie; Xie, Ye-Xiang; Li, Jin-Heng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 39 p. 9909 - 9913
873-66-5
甲基苯乙烯
+
5720-07-0
4-甲氧基苯硼酸
→
反应条件
5912-82-3
反应条件
potassium fluoride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; palladium diacetate; 2,2,2-trimethylacetic acid in tetrahydrofuran T=20°C; Oxidative Heck reaction; 24 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
He, Zhiheng; Kirchberg, Sylvia; Froehlich, Roland; Studer, Armido
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3699 - 3702
14476-62-1
→
反应条件
5912-82-3
反应条件
1: acetic acid; lithium chloride / 24 h / 25 °C 2: palladium diacetate; triphenylphosphine; caesium carbonate / tetrahydrofuran / 5 h / 40 °C / |Inert atmosphere 3: NiCl2(PPh3)2 / tetrahydrofuran / 12 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Yang, Zhaozhen; Chen, Xiaoyi; Kong, Wei; Xia, Siyuan; Zheng, Renwei; Luo, Fang; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 13 p. 2175 - 2185
1449791-47-2
+
100-52-7
苯甲醛
→
反应条件
5912-82-3
反应条件
lithium hydroxide hydrate in tetrahydrofuran T=70°C; 5 h;
参考文献
Guo, Lin; Yang, Chao; Zheng, Lewei; Xia, Wujiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5787 - 5792
1427318-05-5
→
反应条件
5912-82-3
反应条件
1: palladium diacetate; triphenylphosphine; caesium carbonate / tetrahydrofuran / 5 h / 40 °C / |Inert atmosphere 2: NiCl2(PPh3)2 / tetrahydrofuran / 12 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Yang, Zhaozhen; Chen, Xiaoyi; Kong, Wei; Xia, Siyuan; Zheng, Renwei; Luo, Fang; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 13 p. 2175 - 2185
33675-41-1
→
反应条件
5912-82-3
反应条件
1: potassium carbonate / ethanol / 10 h / 50 °C 2: bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl; potassium carbonate / toluene / 10 h / 50 °C / |Inert atmosphere 3: NiCl2((PPh3)P)2 / tetrahydrofuran / 10 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Liu, Ge; Kong, Lichun; Shen, Ji; Zhu, Gangguo
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 14 p. 2310 - 2321
100-06-1
对甲氧基苯乙酮
→
反应条件
5912-82-3
+
1380439-41-7
反应条件
1.1: magnesium / tetrahydrofuran / 20 °C 1.2: Reflux 2.1: sulfuric acid; acetic acid / 3 h / Reflux View Scheme
参考文献
Liu, Hua; Cao, Li; Sun, Jia; Fossey, John S.; Deng, Wei-Ping
Chemical Communications, 2012 , vol. 48, # 21 p. 2674 - 2676
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