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diisobutylaluminium hydride in toluene

1.1: lithium aluminium tetrahydride / diethyl ether / 3 h / |Inert atmosphere; |Reflux 2.1: dihydrogen peroxide / 2,2,2-trifluoroethanol / 1.33 h / 0 - 20 °C / |Inert atmosphere 3.1: triethylamine / ethanol / 0.5 h / 20 °C / |Inert atmosphere 3.2: 2.25 h / 0 - 20 °C 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / -20 - 20 °C / |Inert atmosphere View Scheme

sulfuric acid; dihydrogen peroxide in methanol; water; isopropyl alcohol T=20°C; 3 h;