(2-溴苯基)(4-甲氧基苯基)甲酮合成路线 （共 10 条）
反应条件
in acetonitrile 14 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9786 - 9789
反应条件
4 A molecular sieve; pyridinium chlorochromate in dichloromethane
T=20°C; 2 h;
参考文献
Moorthy, Jarugu Narasimha; Samanta, Subhas
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9786 - 9789
反应条件
aluminium trichloride in chloroform
T=20°C; Friedel-Crafts reaction; 12 h;
参考文献
Treu, Matthias; Jordis, Ulrich
Molecules, 2002 , vol. 7, # 1 p. 18 - 25
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=20°C; 1 h;
参考文献
Okano, Masateru; Amano, Masayuki; Takagi, Kentaro
Tetrahedron Letters, 1998 , vol. 39, # 19 p. 3001 - 3004
反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C
1.2: 58 percent / tetrahydrofuran; hexane / 2 h / -78 °C
2.1: 90 percent / PCC; Florisil / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Katsuno, Mika; Yoshino, Takashi; Arai, Yukari; Hiroya, Kou; Sakamoto, Takao
Tetrahedron, 2007 , vol. 63, # 12 p. 2695 - 2711
反应条件
1.1: n-BuLi / hexane; tetrahydrofuran / 0.5 h / -78 °C
1.2: 58 percent / tetrahydrofuran; hexane / 2 h / -78 °C
2.1: 90 percent / PCC; Florisil / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Inamoto, Kiyofumi; Katsuno, Mika; Yoshino, Takashi; Arai, Yukari; Hiroya, Kou; Sakamoto, Takao
Tetrahedron, 2007 , vol. 63, # 12 p. 2695 - 2711
反应条件
chloroacetic acid anhydride
T=170 - 180°C;
参考文献
Unger
Justus Liebigs Annalen der Chemie, 1933 , vol. 504, p. 267,282
参考文献
Bachmann
Journal of the American Chemical Society, 1932 , vol. 54, p. 1969,1970
Journal of the American Chemical Society, 1933 , vol. 55, p. 1179,1186
反应条件
aluminium trichloride
参考文献
Heidenreich
Chemische Berichte, 1894 , vol. 27, p. 1454
反应条件
in acetonitrile
14 h; Irradiation;
参考文献
Moorthy, Jarugu Narasimha; Samanta, Subhas
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9786 - 9789
