2,3-二氢-2-(碘甲基)苯并呋喃合成路线 （共 6 条）
反应条件
dimethylboron bromide; tetra-(n-butyl)ammonium iodide; triethylamine in dichloromethane T=0°C; 12 h;
参考文献
Gauthier, Jacques Yves; Guindon, Y.
Tetrahedron Letters, 1987 , vol. 28, # 48 p. 5985 - 5988
反应条件
1: sodium azide; copper / N,N-dimethyl-formamide / 90 °C 2: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: 90 percent / HgO, I2 / CH2Cl2 / 96 h / 20 °C 2: 85 percent / NaOH / methanol / 5 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Hatakeyama, Takahiro; Takeo, Mitsuhiro; Suginome, Hiroshi; Tokuda, Masao
Synthesis, 1997 , # 1 p. 23 - 25
反应条件
iodine; tin(IV) chloride in dichloromethane
24 h; Ambient temperature;
参考文献
Orito, Kazuhiko; Hatakeyama, Takahiro; Takeo, Mitsuhiro; Suginome, Hiroshi; Tokuda, Masao
Synthesis, 1997 , # 1 p. 23 - 25
反应条件
1: 210 °C / Microwave irradiation
2: iodine / ethanol; water / 12 h / 50 °C
View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
反应条件
1: potassium carbonate / acetone / Reflux
2: 210 °C / Microwave irradiation
3: iodine / ethanol; water / 12 h / 50 °C
View Scheme
参考文献
Chen, Wen; Yang, Xiao-Dong; Li, Yan; Yang, Li-Juan; Wang, Xue-Quan; Zhang, Gao-Lan; Zhang, Hong-Bin
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 11 p. 4250 - 4255
