反应条件
1.1: ethanethiol; n-butyllithium / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 2 h / 0 - 70 °C / |Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C
2.2: 2 h / 0 - 20 °C
3.1: ethanethiol; n-butyllithium / N,N,N',N',N'',N''-hexamethylphosphoric triamide / 2 h / 0 - 70 °C / |Inert atmosphere
View Scheme
参考文献
Zhang, Wen-Jing; Wu, Jing-Fang; Zhou, Peng-Fei; Wang, Yang; Hou, Ai-Jun
Tetrahedron, 2013 , vol. 69, # 29 p. 5850 - 5858
