diethyl ether Erwaermen des Reaktionsprodukts mit wss.Kalilauge;

in water

暂无反应条件数据

acetic anhydride

sodium hydroxide; acetic anhydride 1.) from 75 deg C to 80 deg C, 2 h, 2.) RT; Yield given. Multistep reaction;

sodium methylate

sulfuric acid; sodium nitrite

1: 1.) acetic anhydride, 2.) 10percent NaOH / 1.) from 75 deg C to 80 deg C, 2 h, 2.) RT 2: 1.) 20percent NaOH / 1.) EtOH, 50 deg C, 2.) EtOH, reflux, 2 h 3: 79 percent / NaNO2, 42percent AcOH / H2O / 0.17 h / 60 °C 4: 60 percent / H2 / PtO2 / methanol / 0.5 h / 2068.6 Torr 5: 64 percent / 1 h / Heating 6: 87 percent / 10percent NaOH / 0.33 h / Heating View Scheme