1: With iodine; zinc in diethyl ether Reformatsky reaction; 4 h; Inert atmosphereReflux; 2: With hydrogenchloride in diethyl ether; water T=0°C; Inert atmosphere; 3: With magnesium sulfate; toluene-4-sulfonic acid in toluene 7 h; Inert atmosphereReflux;
参考文献
Petroski, Richard J.; Bartelt, Robert J.; Vermillion, Karl
Synthetic Communications, 2009 , vol. 39, # 8 p. 1389 - 1405