in cyclohexane T=20°C; Photolysis; Product distribution; Further Variations:reaction times;
参考文献
Journal of Organic Chemistry, , vol. 72, # 23 p. 8700 - 8706
→
反应条件
in acetonitrile-D3 Kinetics; Complex and allyl bromide was added to an NMR tube which contained CD3CN, after the soln. was degassed, the sealed NMR tube with a reflux condenser was thermostated at 353 K for 0.5 h;; Detected by NMR-spectroscopy at 298 K; the organic products were analysed by GLC;;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 563 - 570
→
反应条件
in acetonitrile-D3 Kinetics; Complex and allyl bromide was added to an NMR tube which contained CD3CN, after the soln. was degassed, the sealed NMR tube with a reflux condenser was thermostated at 353 K for 30 h;; Detected by NMR-spectroscopy at 298 K; the organic products were analysed by GLC;;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 563 - 570
→
反应条件
in benzene decompn. at 100°C under N2;
参考文献
Journal of Molecular Catalysis, , vol. 58, p. 95 - 106
in acetonitrile-D3 Kinetics; byproducts: C4H8; Complex and allyl bromide was added to an NMR tube which contained CD3CN, after the soln. was degassed, the sealed NMR tube with a reflux condenser was thermostated at 353 K for 100 h;; Detected by NMR-spectroscopy at 298 K; the organic products were analysed by GLC;;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 563 - 570
in acetonitrile-D3 Kinetics; Complex and allyl bromide was added to an NMR tube which contained CD3CN, after the soln. was degassed, the sealed NMR tube with a reflux condenser was thermostated at 353 K for 0.5 h;; Detected by NMR-spectroscopy at 298 K; the organic products were analysed by GLC;;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 563 - 570
in acetonitrile-D3 Kinetics; Complex and allyl bromide was added to an NMR tube which contained CD3CN, after the soln. was degassed, the sealed NMR tube with a reflux condenser was thermostated at 353 K for 30 h;; Detected by NMR-spectroscopy at 298 K; the organic products were analysed by GLC;;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 2 p. 563 - 570