1-(2,4-二羟基苯基)-2-对甲苯乙酮合成路线 (共 4 条)
反应条件
boron trifluoride diethyl etherate
T=100°C; Friedel-Crafts acylation; 2 h;
参考文献
Kim, Young-Woo; Brueggemeier, Robert W
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6113 - 6115
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride
und Kochen des Reaktionsprodukts mit Wasser;
参考文献
Chapman; Stephen
Journal of the Chemical Society, 1923 , vol. 123, p. 408
反应条件
1: 1-(2,4-dihydroxyphenyl)-2-(4'-methylphenyl)-ethanone With boron trifluoride diethyl etherate in N,N-dimethyl-formamide
T=55°C; Inert atmosphere;
2: N,N-dimethyl-formamide With methanesulfonyl chloride
T=55 - 80°C; 3 h; Inert atmosphere;
参考文献
Yeap, Guan-Yeow; Yam, Wan-Sinn; Dominiak, Paulina; Ito, Masato M.
Journal of Molecular Structure, 2010 , vol. 967, # 1-3 p. 25 - 33
反应条件
morpholine in isopropyl alcohol
T=80°C;
参考文献
Gao, Guang-Yao; Li, Dian-Jun; Keung, Wing Ming
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4069 - 4081