3-(4-甲基磺酰基-苯基)-1-丙醇合成路线 （共 5 条）
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran
T=20°C; 1 h; Inert atmosphere;
参考文献
Szostak, Michal; Spain, Malcolm; Procter, David J.
Organic Letters, 2012 , vol. 14, # 3 p. 840 - 843
反应条件
1: 100 mg / H2 / Pd/C / ethyl acetate; ethanol / 168 h / 20 °C
2: 4.25 g / aq. H2SO4 / CH2Cl2 / Heating
3: 2.72 g / LiAlH4 / diethyl ether
View Scheme
参考文献
Tachikawa, Takashi; Yoshida, Akihiro; Tojo, Sachiko; Sugimoto, Akira; Fujitsuka, Mamoru; Majima, Tetsuro
Chemistry - A European Journal, 2004 , vol. 10, # 21 p. 5345 - 5353
反应条件
1: 16.85 g / piperidine; pyridine / 3 h / Heating
2: 100 mg / H2 / Pd/C / ethyl acetate; ethanol / 168 h / 20 °C
3: 4.25 g / aq. H2SO4 / CH2Cl2 / Heating
4: 2.72 g / LiAlH4 / diethyl ether
View Scheme
参考文献
Tachikawa, Takashi; Yoshida, Akihiro; Tojo, Sachiko; Sugimoto, Akira; Fujitsuka, Mamoru; Majima, Tetsuro
Chemistry - A European Journal, 2004 , vol. 10, # 21 p. 5345 - 5353
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Tachikawa, Takashi; Yoshida, Akihiro; Tojo, Sachiko; Sugimoto, Akira; Fujitsuka, Mamoru; Majima, Tetsuro
Chemistry - A European Journal, 2004 , vol. 10, # 21 p. 5345 - 5353
反应条件
C62H52ClFeN2O2; dihydrogen peroxide in water
T=0°C; 6 h; enantioselective reaction;
参考文献
Egami, Hiromichi; Katsuki, Tsutomu
Synlett, 2008 , # 10 p. 1543 - 1546
