您好,欢迎来到魔法化学网!
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
59211-64-2
合成路线
(共 20 条)
99-90-1
4-溴苯乙酮
+
126747-14-6
4-氰基苯硼酸
→
反应条件
59211-64-2
反应条件
5 palladium on charcoal; potassium carbonate in ethanol; water T=80°C; Suzuki Coupling; 0.333333 h;
参考文献
Liu, Chun; Rao, Xiaofeng; Zhang, Yixia; Li, Xinmin; Qiu, Jieshan; Jin, Zilin
European Journal of Organic Chemistry, 2013 , # 20 p. 4345 - 4350
99-90-1
4-溴苯乙酮
+
126747-14-6
4-氰基苯硼酸
→
反应条件
1591-30-6
4,4'-联苯甲腈
+
59211-64-2
反应条件
1: With [resin-CH2N(CH3)3]2CO3; Pd(PAnPh2)2Cl2 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
参考文献
Lan, Ping; Berta, Daniela; Porco Jr., John A.; South, Michael S.; Parlow, John J.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9678 - 9686
66107-32-2
三氟甲磺酸4-氰基苯基醚
+
171364-81-1
4-乙酰苯基硼酸,醇酯
→
反应条件
59211-64-2
反应条件
potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 16 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
→
反应条件
59211-64-2
反应条件
potassium carbonate; palladium diacetate; triphenylphosphine in methanol T=70°C; 16 h;
参考文献
Molander, Gary A.; Petrillo, Daniel E.
Journal of the American Chemical Society, 2006 , vol. 128, # 30 p. 9634 - 9635
3058-39-7
4-碘氰基苯
+
149104-90-5
→
反应条件
59211-64-2
反应条件
potassium fluoride; potassium carbonate in water T=100°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Bernini, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Forte, Giovanni; Petrucci, Francesco; Prastaro, Alessandro; Niembro, Sandra; Shafir, Alexandr; Vallribera, Adelina
Green Chemistry, 2010 , vol. 12, # 1 p. 150 - 158
→
反应条件
59211-64-2
反应条件
potassium phosphate; 2BF4(1-)*C42H38Fe2N6O2Pd2(2-) in water; acetonitrile T=100°C; Suzuki cross coupling; 2 h; Inert atmosphere;
参考文献
Das, Raj K.; Saha, Biswajit; Rahaman, S. M. Wahidur; Bera, Jitendra K.
Chemistry - A European Journal, 2010 , vol. 16, # 48 p. 14459 - 14468
5731-01-1
4-乙酰基-4-溴代联苯
→
反应条件
59211-64-2
反应条件
dichloro[bis{1-(dicyclohexylphosphanyl)piperidine}]palladium; sodium carbonate in 1-methyl-pyrrolidin-2-one T=140°C; 6 h; Inert atmosphere;
参考文献
Gerber, Roman; Oberholzer, Miriam; Frech, Christian M.
Chemistry - A European Journal, 2012 , vol. 18, # 10 p. 2978 - 2986
64101-67-3
+
126747-14-6
4-氰基苯硼酸
→
反应条件
59211-64-2
反应条件
potassium phosphate; BF4(1-)*C31H33ClN5Ni(1+) in ethylene glycol dimethyl ether T=120°C; Suzuki-Miyaura coupling; 48 h; Inert atmosphereSealed tube;
参考文献
Kuroda, Jun-Ichi; Inamoto, Kiyofumi; Hiroya, Kou; Doi, Takayuki
European Journal of Organic Chemistry, 2009 , # 14 p. 2251 - 2261
→
反应条件
59211-64-2
反应条件
1: para-bromobenzonitrile With chloro-trimethyl-silane; tributoxyborane; magnesium; ethylene dibromide; lithium chloride in tetrahydrofuran T=25°C; 1 h; Inert atmosphere; 2: para-bromoacetophenone With 1,1'-bis-(diphenylphosphino)ferrocene; caesium carbonate; palladium dichloride in tetrahydrofuran; ethanol; N,N-dimethyl-formamide T=65°C; Suzuki-Miyaura cross coupling reaction; 12 h; Inert atmosphere;
参考文献
Haag, Benjamin A.; Saemann, Christoph; Jana, Anukul; Knochel, Paul
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7290 - 7294
99-91-2
对氯苯乙酮
+
126747-14-6
4-氰基苯硼酸
→
反应条件
59211-64-2
反应条件
5 palladium on charcoal; SIPr*HCl; sodium hydroxide; phosphorous acid trimethyl ester in ethanol T=80°C; Suzuki Coupling; 5 h; Inert atmosphere;
参考文献
Ke, Haihua; Chen, Xiaofeng; Zou, Gang
Applied Organometallic Chemistry, 2014 , vol. 28, # 1 p. 54 - 60
1
2
下一页
末页
到第
页
确定