(9CI)-2-(3-甲基-1-哌嗪)-嘧啶合成路线 （共 3 条）
反应条件
triethylamine in chloroform
T=25°C; 4 h;
参考文献
Euro-Celtique, S.A.
Patent: WO2004/29044 A1, 2004 ;
Location in patent: Page 240 ;
反应条件
acetyl chloride in dichloromethane
T=20°C; 24 h;
参考文献
GRAUERT, Matthias; BISCHOFF, Daniel; DAHMANN, Georg; KUELZER, Raimund; RUDOLF, Klaus; WELLENZOHN, Bernd
Patent: US2013/150341 A1, 2013 ;
Location in patent: Paragraph 0350; 0351 ;
反应条件
1: 2 h / 120 °C
2: acetyl chloride / dichloromethane / 24 h / 20 °C
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参考文献
GRAUERT, Matthias; BISCHOFF, Daniel; DAHMANN, Georg; KUELZER, Raimund; RUDOLF, Klaus; WELLENZOHN, Bernd
Patent: US2013/150341 A1, 2013 ;
