1-(5-溴噻吩-3-基)乙酮合成路线 （共 4 条）
反应条件
bromine; sodium acetate in acetic acid Ambient temperature;
参考文献
Karlsson, Olle
Synthetic Communications, 1981 , vol. 11, # 1 p. 29 - 34
反应条件
1: With sodium acetate; acetic acid T=20°C; 0.166667 h; 2: With bromine T=0°C; 2 h;
参考文献
WO2014/31784 A1, ;
Paragraph 0546 ;
反应条件
in acetic acid T=20°C; activation energy; Rate constantThermodynamic data;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 27, # 6 p. 538 - 539
反应条件
1: toluene-p-sulphonic acid / benzene / 20 h / Heating
2: n-BuLi / diethyl ether / -70 - -15 °C
View Scheme
参考文献
Noto, Renato; Lamartina, Liliana; Arnone, Caterina; Spinelli, Domenico
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 689 - 694
